Introduction
The power density of a gearbox is an important consideration for many applications and is especially important for gearboxes used on aircraft. One factor that limits gearbox power density is the need to transmit power for the required number of cycles while avoiding gear surface fatigue failure (micropitting, pitting, or spalling). Effective and economical methods for improving surface fatigue lives of gears are therefore highly desirable. Thin, hard coatings have potential for improving gear performance. In fact, coatings are reported to have some successful applications [1-3] where product durability improvements have been achieved by the application of thin, hard coatings to gears.
Diamond-like carbon and related materials have the potential for a wide variety of applications that require wear protection and/or low-friction properties. Because of the widely recognized potential, the deposition methods and resulting properties of the films have been studied extensively [4-6]. Today’s deposition technology allows for the production of a great diversity of coatings, but the ability to tailor the tribological behavior of a coating for a particular application has been elusive.
Aerospace gearing requirements are demanding, calling for high power density, long life, and excellent reliability. The low friction properties and high hardness of diamond-like and related coatings offer the possibility to improve the performance of aerospace gearing. Naik, et al [7] tested the adherence and toughness of two coatings using both disk-on-rod rolling-contact and gear tests, and they reported promising results. Alanou, et al [8] found that coatings could increase the scuffing load capacity of rolling and sliding disks used to simulate aerospace gearing contacts, but they also reported poor adherence for one particular substrate and coating combination. Joachim, Kurz, and Glatthaar [3] reported promising results of evaluations of tungsten carbon carbide and amorphous boron carbide coatings using laboratory tests, but they also report mixed results when applying such coatings to commercial applications.
The purpose of the present investigation was to compare the surface fatigue lives of coated and uncoated gears using accelerated life tests. The testing is considered as accelerated in that the contact stresses used for testing exceeds the stresses used for design of the target application (helicopter gearing). The metal-containing, carbon-based, diamond-like (Me-DLC) coating selected for this study was designed specifically for the aerospace gearing applications.
Description of the Test Gears, Lubricant, and Coating
The test gears used for this work were manufactured in one lot from a single heat of consumable-electrode, vacuum-melted (CVM) AISI 9310 steel. The nominal chemical composition of the AISI 9310 material is given in Table 1. The gears were case carburized and heat treated according to Table 2. Figure 1 is a photomicrograph of an etched and polished gear tooth showing the case and core microstructure of the test gears. The nominal properties of the carburized gears were a case hardness of Rockwell C60, a case depth of 0.97 mm (0.038 in.), and a core hardness of Rockwell C38. The test gears were a subset of a larger lot of gears that were used by Townsend and Shimski [9] to study the influence of elastohydrodynamic film thickness and extreme pressure additives on gear surface fatigue life.
The dimensions for the test gears are given in Table 3. The gear pitch diameter was 89 mm (3.5 in.,) and the tooth form was a 20° involute profile modified to provide a tip relief of 0.013 mm (0.0005 in.) starting at the highest point of single tooth contact. The gear tooth surface finish after final grinding was specified as a maximum of 0.406 µm (16 µin.) root-mean-squared (r.m.s.).
The lubricant used for testing was from a single batch of synthetic paraffinic oil. Physical properties of this lubricant are summarized in Table 4. Five percent of extreme pressure additive with partial contents including phosphorus and sulfur was added to the lubricant. This lubricant and additive combination has been used extensively for gear fatigue testing in the NASA Glenn spur gear fatigue rigs. For example, Krantz [10] reported 146 tests using this same oil (termed “NASA standard” in the referenced article) to evaluate the surface fatigue lives of AISI 9310 steel gears. The oil and additive mixture used in this work is similar to five-centistoke oils used for helicopter main gearboxes. The film thickness at the pitch point for the operating conditions of the surface fatigue testing was calculated using the computer program EXTERN. This program, developed at the NASA Glenn Research Center, is based on the methods of Anderson, Lowenthal, and Black [11,12]. For the purposes of the calculation, the gear surface temperature was assumed to be equal to the average oil outlet temperature. This gave a calculated pitch-line film thickness of 0.54 µm (21 µin.).
W(tungsten)-DLC coatings were deposited onto carburized spur gears after final grinding, by using an unbalanced magnetron sputter deposition process, at a deposition temperature of approximately 200°C [13]. Prior to coating deposition, the spur gears were “vapor honed” using pressurized water-based media containing ∼10 µm diameter Al2O3 particles. The coating/gear system consisted of an elemental Cr (chromium) adhesion layer adjacent to the steel substrate, followed by an intermediate transition region, featuring alternating lamellae composed of Cr and WC, and an outermost W-containing hydrocarbon (W-C:H) layer. The composition of the outermost W-C:H layer, in atomic percent, has been determined via secondary ion mass spectrometry (SIMS) to be approximately 12 percent W, 70 percent C, 15 percent H, and 3 percent Ni, which forms the binder element for the WC sputter targets [14].
Measurements of the properties of Me-DLC coating materials are sparse, primarily on W-DLC coatings [15-18]. The Young’s modulus of the DLC coating is in the range 100-120 GPa as measured using beam curvature [15, 16] and instrumented indentation [17, 18] methods. W-DLC deposited on steel is in residual compression. Measurements performed by beam curvature indicate a stress, σR ≈ -900 MPa [15]; the amorphous nature of the Me-DLC coating [19, 20] precludes stress measurement through the application of x-ray diffraction methods. The fracture toughness of the W-DLC has been determined from the critical strain for channel cracking [15] as: ΓDLC ≈ 35Jm-2. The toughness of the interface between the W-DLC coating and the steel substrate in the presence of a Cr adhesion layer has been shown to be well in excess of that for the Me-DLC coating, itself [15]. This high toughness eliminates the interface as a weak link and distinguishes the present systems from those with weak interfaces.
Test Apparatus and Procedure
The gear fatigue tests were performed in the NASA Glenn Research Center’s gear test apparatus. The test rig is shown in Figure 2 (a) and described in reference [21]. The rig uses the four-square principle of applying test loads, and thus the input drive only needs to overcome the frictional losses in the system. The test rig is belt driven and operated at a fixed speed of 10 000 r.p.m. for the duration of a particular test.
A schematic of the apparatus is shown in Figure 2(b). Oil pressure and leakage replacement flow is supplied to the load vanes through a shaft seal. As the oil pressure is increased on the load vanes located inside one of the slave gears, torque is applied to its shaft. This torque is transmitted through the test gears and back to the slave gears. In this way power is circulated, and the desired load and corresponding stress level on the test gear teeth may be obtained by adjusting the hydraulic pressure. The two identical test gears may be started under no load, and the load can then be applied gradually. This arrangement also has the advantage that changes in load do not affect the width or position of the running track on the gear teeth. To enable testing at the desired contact stress, the gears are tested with the faces offset, as shown in Figure 2. By utilizing the offset arrangement for both faces of the gear teeth, a total of four surface fatigue tests can be run for each pair of gears.
Separate lubrication systems are provided for the test and slave gears. The two lubrication systems are separated at the gearbox shafts by pressurized labyrinth seals, with nitrogen as the seal gas. The test gear lubricant is filtered through a 5-µm (200-µin.) nominal fiberglass filter.
A vibration transducer mounted on the gearbox is used to automatically stop the test rig when the broadband r.m.s. vibration magnitude increases beyond a threshold, indicating that gear surface fatigue damage has occurred. The gearbox is also automatically stopped if there is a loss of oil flow to either the slave gearbox or the test gears, if the test gear oil overheats, or if there is a loss of seal gas pressurization.
The test gears were run with the tooth faces offset by a nominal 3.3 mm (0.130 in.) to give a surface load width on the gear face of 3.0 mm (0.120 in). The actual tooth face offset for each test is based on the measured face width of the test specimen, and the offset is verified upon installation using a depth gage. The nominal 0.13-mm- (0.005-in.-) radius edge break is accounted for to calculate load intensity. All tests were run-in at a load (normal to the pitch circle) per unit width of 123 N/mm (700 lb/in.) for one hour. The load was then increased to the desired test load. For the uncoated gears, all tests were conducted using a test load of 580 N/mm (3300 lb/in.), which resulted in a 1.7-GPa (250-ksi) pitch-line maximum Hertz stress. For the coated gears, six tests were conducted at the same test load as was used for the uncoated gears while eight tests were conducted using a test load of 720 N/mm (4100 lb/in.) which resulted in a 1.9-GPa (280-ksi) pitch-line maximum Hertz stress. The Hertz stress just stated is an idealized stress index assuming static equilibrium, perfectly smooth surfaces, and an even pressure distribution across a 2.79 mm (0.110 in.) line contact (the line length is less than the face width allowing for the face offset and the radius edge break).
Typical dynamic tooth forces using the same rigs and gears of the same specification have been measured (Krantz, [10]), and the results are provided in Figure 3. The tooth forces reported in Fig. 3 are the dynamic forces normal to the tooth surface for a nominal pitch-line test load intensity of 580 N/mm (3300 lb/in.). The contact force used for stress calculations for such load intensity was 1720 N (387 lb). This value for the contact force is the value required for static equilibrium, and it is somewhat less than the measured dynamic forces.
The gears were tested at 10 000 rpm, which gave a pitch-line velocity of 46.5 m/s (9154 ft/min). Inlet and outlet oil temperatures were continuously monitored. Cooled lubricant was supplied to the inlet of the gear mesh at 0.8 liter/min (0.2 gal/min) and 320±7 K (116±13 °F). The lubricant outlet temperature was recorded and observed to have been maintained at 348±4.5 K (166±8 °F). The lubricant was circulated through a 5-µm- (200-µin. -) nominal fiberglass filter to remove wear particles. For each test, 3.8 liter (1 gal) of lubricant was used. The tests ran continuously (24 hr/day) until a vibration detection transducer automatically stopped the rig. The transducer is located on the gearbox housing. The gears were also inspected visually at intervals of approximately 50 million cycles. For purposes of this work, surface fatigue failure was defined as one or more spalls or pits covering at least 50 percent of the width of the Hertzian line contact on any one tooth. If the gear pairs operated for more than 460 hours (corresponding to 275 million stress cycles) without failure, the test was suspended.
Test Results and Discussion
Results of the gear surface fatigue testing are summarized in Table 5. A total of 29 tests were completed, 15 tests using the uncoated gears and 14 tests using the coated gears. All of the baseline tests were conducted at a Hertzian stress index of 1.7 Gpa (250 ksi), with all tests resulting in failures. The range of duration for the tests using uncoated baseline gears was 25-272 million revolutions. The coated gears were tested at two loads. Six of the coated gears were tested at a Hertzian stress index of 1.7 GPa (250 ksi), and eight of the coated gears were tested at a stress index of 1.9 GPa (280 ksi). The range of duration for the tests using coated gears was 63-311 million revolutions, and 11 of the 14 tests were completed with no failure after at least 275 million revolutions.
The distributions of the fatigue lives were modeled as two-parmeter Weibull distributions (Weibull, [22] and Hallinan, [23]). The fatigue lives are system lives, the system consisting of two identical gears. Tests that were suspended after pre-specified times showed no signs of impending failure, and so such tests were treated as right-censored life tests for the purpose of statistical analysis. It was decided not to estimate the slope of the coated gear population with only three failure data points. Instead, it was assumed that the coated and uncoated gears had life distributions with equal Weibull slope parameters. A likelihood ratio statistical test (Meeker and Escobar, [24]) was used to verify that the assumption of equal slopes was indeed a reasonable assumption. Software employing the maximum likelihood method (Krantz, [25]) was used to estimate the Weibull parameter values from the test data. Figure 4 is a Weibull plot displaying the test data and the lines representing the maximum likelihood fit Weibull distributions. Data points are plotted at the positions of exact median ranks (Jaquelin, [26]) with adjustments to the order numbers to account for suspended tests (Johnson, [27]). The results of the statistical analysis are summarized in Table 6. The 10-percent lives of the uncoated and coated gear populations were estimated to be 28×106 and 180×106 cycles, respectively.
From the data plot and the statistical analysis, it is clear that the lives of the coated gears were longer than the lives of the uncoated gears by a factor of approximately six. To test that the measured life difference was a statistically significant one, the null hypothesis was set forth that the coated and uncoated gears represented a single fatigue life population. If the null hypothesis were true, the observed life difference would have come about from random sampling effects. The null hypothesis was tested using the likelihood ratio method (Meeker and Escobar, [24]), and it was found that the null hypothesis can be rejected with greater than 99.5-percent confidence, a statistically significant difference.
The preceding text provides a quantitative assessment of the influence of the coating on gear surface fatigue life. One can also make a qualitative comparison to other gear fatigue studies that have been conducted using the same test rigs, the same test procedure, the same gear material, and the same lubricant. Table 7 provides a compilation of gear fatigue test data gathered from references [28-32]. The table is sorted by the measured 10-percent life, except the gears of the present study occupy the last two rows of the table. The measured fatigue lives of the uncoated-baseline gears of the present study are consistent with the historical database for the AISI 9310 gear steel. The coating used for the present study provided for significantly longer surface fatigue lives of the gear tooth surfaces. The coating performance is especially impressive keeping in mind that for the coated gears, eight of the 14 tests were conducted at a higher Hertzian stress (1.9 GPa) than was the stress (1.7 GPa) for the other tests reported in Table 7.
Figure 5 provides images of the tested gears showing tested surfaces with fatigue failures. The figure shows typical features of the failed surfaces, and regardless if the gear was coated or uncoated the pitted teeth had similar features. For both the uncoated and coated surfaces, the surface topography changes with running. The surfaces take on a smoother appearance, and there is evidence of wear. By subjective evaluation, it appears that the total amount of wear on the coated surfaces is less than that of the uncoated surfaces. Because of the face-offset testing method, there remains in the middle of a tested gear a thin track of tooth surface that was not in contact. Tracing across a tested tooth surface using a soft stylus, one can feel a clear wear step on the uncoated gears. Such a step could not be detected on the coated and tested gears. One could speculate that the longer fatigue lives of the coated gears were a result of the wear protection offered by the coating. Such a mechanism has been stated as an explanation for an increase of fatigue lives for bearings due to providing a coating to rolling elements of bearings (Olofsson, et al, Ref. [33]). It has been speculated in the literature that improved durability of coated surfaces can in some cases be attributed to a polishing mechanism (Polonsky, et al, Refs. [34,35]). That is, one can consider that the surfaces polish one another during initial running. Some guidance concerning the abrasive and polishing characteristics of hard coatings can be found in the literature (Refs. [36-39]). Based on data from these studies, it is likely that the running-in and polishing of micro-scale features of the coated surface occurred during a fraction of the total running times of the gears.
The increased surface fatigue lives due to polishing (or superfinishing) of uncoated, high quality, ground gears has been clearly established (Refs. [10, 40, 41]). It has been speculated that the increase of surface fatigue lives for superfinished gears might be due to reductions of asperity interactions (Refs. [10, 42]). It is considered likely that for coated gears, the changes to the topography of the tooth surface during running plays an important role concerning the surface fatigue.
To help characterize the running-in characteristics of the coated and tested gears, a tested gear was inspected using a scanning-electron microscope. Figure 6 shows typical features at three levels of resolution. At low resolution (Figure 6a), one can see traces of the grinding marks, indicating that the coating thickness was uniform enough such that application of the coating did not significantly change the surface topography. Figure 6a) also shows the contact pattern, with the run-in portion of the surface appearing as slightly darker than the un-run portion of the surface. Figure 6(b) shows a portion of the surface of Figure 6a at a somewhat higher resolution. It appears that the coating has been smoothed and/or removed (darker areas) along certain grinding-mark features. Figure 6c shows the same portion of the tooth at a still higher resolution. The spherical shape of the coating micro-structure is evident, and a portion of the surface has been smoothed. By using backscatter electron micrographs and energy dispersive x-ray spectrums, it was found that in localized areas the coating had been removed from the surface.
Summary
The purpose of the present investigation was to compare the surface fatigue lives of coated and uncoated gears using accelerated life tests. The test gears used were manufactured in one lot from a single heat of consumable-electrode, vacuum-melted (CVM) AISI 9310 steel. The gears were case-carburized and ground to aerospace quality. A subset of the ground gears was provided with a thin, hard, low-friction coating by magnetron sputtering, a physical vapor deposition (PVD) process. The coating that was applied to the gears was a metal-containing, carbon-based (Me-DLC) coating. Tests were conducted using a four-square type gear fatigue rig. Tests were run until either a surface fatigue failure of any one gear tooth or until a predetermined number of cycles had occurred with no failure. The following specific results were obtained:
- Fifteen tests were completed using the uncoated gears, using a load intensity corresponding to a Hertzian stress index of 1.7 GPa (250 ksi).
- Fourteen tests were completed using the coated gears. Two load intensities were used for the coated gears, with six tests conducted at a Hertzian stress index of 1.7 GPa (250 ksi) and eight tests conducted at a stress index of 1.9 GPa (280 ksi).
- For the uncoated gears, all tests resulted in failure with test durations ranging from 25-272 million revolutions.
- For the coated gears, three of the tests resulted in failure, while 11 tests were suspended without failure. The testing durations ranged from 63-311 million revolutions.
- The distributions of the fatigue lives were modeled as two-parmeter Weibull distributions. From the Weibull analysis, the 10-percent lives of the uncoated and coated gear populations were estimated to be 28×106 and 180×106 cycles, respectively.
- The measured life difference is a statistically significant difference to a greater than 99.5 percent statistical confidence.
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