The low-pressure carburizing and high-pressure gas quenching process offers a significant potential for advanced distortion control where the gas-quenching process provides a more homogenous heat-transfer coefficient on the surface of the quenched components when compared to quenching with liquids such as oil or polymers.

In many applications the high demands regarding fatigue properties of transmission components can be reached only by the application of customized case hardening. This case-hardening process results in a wear resistant surface layer in combination with a tough core.

However, as a side effect, the components get distorted during heat treatment. This distortion has a significant cost impact because distorted components need to be hard machined after heat treatment. Therefore, the proper control of distortion and the variation of distortion is an important measure to minimize production costs.

By applying the technology of low-pressure carburizing (LPC) and high-pressure gas quenching (HPGQ), heat-treat distortion can be significantly reduced. Especially for e-drive components, significant cost-savings can be achieved compared to other process-combinations such as atmospheric carburizing with oil quenching.

HPGQ provides a very uniform heat-transfer coefficient. The predictability of movement during quenching is more certain and uniform throughout the load. Further improvements can be achieved by optimizing the gas-quenching parameters. Proper fixturing is another factor for distortion control. Modern CFC materials (carbon-reinforced carbon) are well suited as fixture material for gas quenching. When compared to traditional alloy, CFC demonstrates no deflection or distortion after many subsequent years of use.

This article provides insight into distortion values of transmission components for various applications after optimizing process parameters and the design of heat-treatment fixtures.

1 Introduction

Distortion control is one of the major challenges in modern manufacturing. Distorted gear components cause noise in the transmission and may even create problems during transmission assembly. Especially battery-operated electric vehicles (BEV) and other electrified vehicles (such as hybrids) require a low-noise transmission with high-precision components.

Distortion has a strong cost impact because distorted components often need to be hard machined after heat treatment.

Better control of distortion means:

  • Less cycle time per part in hard machining.
  • Less hard-machining capacity needed.
  • Less tooling cost for hard machining.

With an excellent control of distortion for some applications, hard machining can be completely eliminated. For some other applications, the use of a cost-intensive press quench can be eliminated if an excellent distortion control is established.

1.1 Distortion mechanisms

The plastic deformation of metallic components during heat treatment is referred to as distortion. Distortion occurs if the stress in the material exceeds the yield stress of the material. During case hardening, the components are exposed to high temperatures in the range of 880°C to 1,050°C, and the yield stress decreases strongly with increasing temperature of a component. Three different types of stress in the material need to be distinguished:

Residual stresses (They are induced before heat treatment by casting, forging, machining, etc.) [1]

Thermal stresses (They are caused by the temperature gradient while heating and quenching.)

Transformation stresses (They are caused by the transformation from ferrite to austenite during heating and transformation from austenite to martensite/bainite during quenching.)

These three types of stresses overlay with each other and add up to the total stress in the component. They are influenced by part geometry, steel grade, casting, forging, machining, etc., and they are influenced by the heat treatment. If the total stress in the component exceeds the yield stress, then plastic deformation (distortion) of the component takes place. The chronology and the height of the three types of stresses leading to distortion are dependent on numerous influencing factors, see Figure 1.

Figure 1: Factors influencing distortion.

When analyzing distortion, it should be distinguished between size change and form change. Size change refers to the homogenous growth or shrinkage of the treated component while maintaining its shape (e.g., the homogenous growth or shrinkage of the diameter or the length of the component). Form change refers to a change of the shape of the part (e.g., roundness of a gear, bending of a gear shaft, or deformation of gear-tooth geometry).

All carburized components will have some size change due to the transformation of microstructure from ferrite into martensite. The size change must be controlled with green machining. For example, if an outside diameter grows 10 microns during heat treat, it should be machined 10 microns smaller before heat treatment.

There are many different characteristics affected by form change. However, it helps to better understand form change by simplifying distortion into two main parameters: flatness and roundness.

Form change for shafts is mainly straightness. When analyzing gears, flatness can be determined by the amount of “helix variation,” or “lead variation.” Roundness is a measurement of “circularity.”

Helix average also changes during heat treat. The helix average changes in a minus direction, meaning the tooth is unwinding. For instance, the helix angle may be 15 degrees in the green state, but it may change to 14 degrees after heat treat. This must be compensated with green machining.

1.2 Low pressure carburizing in combination with high pressure gas quenching

By applying the technology of low-pressure carburizing (LPC) and high-pressure gas quenching (HPGQ), heat-treat distortion can be reduced significantly. LPC is a case-hardening process performed in a pressure of only a few millibars using acetylene as the carbon source. During HPGQ, the load is quenched using an inert gas stream instead of a liquid quenching media. Usually, nitrogen or helium is used as a quench gas [2,3,4].

HPGQ offers a significant potential to reduce heat-treat distortion. Conventional quenching technologies such as oil or polymer quenching exhibit inhomogeneous cooling conditions. Three different mechanisms occur during conventional liquid quenching: film boiling, bubble boiling, and convection. The distribution of the local heat-transfer coefficients on the surface of the component is very inhomogeneous as a result of these three mechanisms. These inhomogeneous cooling conditions cause high thermal and transformation stresses in the component and subsequent distortion. During HPGQ, only convection takes place, which results in much more homogenous cooling conditions, see Figure 2 [5, 6]. Significant reductions of distortion by substituting oil quench with HPGQ have been published [7, 8].

Figure 2: Heat-transfer coefficient and temperature distribution in liquid- and gas-quenching [5].

Another advantage of HPGQ is the possibility to adjust the quench intensity exactly to the needed severity by choosing quench pressure and quench velocity. Typical quench pressures range from 2 bar to 20 bar. The gas velocity is controlled by a frequency converter. Typical gas velocities range from 2 m/s to 20 m/s. Quench pressure and gas velocity are chosen depending on the part geometry and the steel grade of the component to achieve optimum results.

The following equation describes the heat-transfer coefficient as a function of gas velocity, gas density and the type of gas [2]:

where

C is constant factor (depending on quench cell).

w is gas velocity.

ρ is gas density.

d is diameter of component.

η is viscosity of the gas.

cp is specific heat capacity of the gas.

λ is thermal conductivity of the gas.

Typical gases applied for HPGQ are nitrogen and helium [2]. To achieve the required core hardness in gears of low-alloyed case hardening steels, helium as a quenching medium and a gas pressure of 20 bar is necessary for many applications.

For many applications, it is not the absolute height of distortion causing manufacturing problems but the spread of distortion. The spread of distortion cannot be compensated with green machining. So, for many applications, the challenge is to optimize the HPGQ in such a way that it provides a heat-treatment process with very little variation of distortion within a load and, over time, from load to load.

2 Strategies for distortion control when applying HPGQ

As described earlier, the gas-quenching process offers two major advantages when compared to liquid quenching in terms of distortion control:

  • More homogenous heat-transfer coefficient around the surface of the quenched component.
  • The flexibility to tailor the quench intensity, specifically for the needs of the quenched component.

To fully exploit the benefits of HPGQ, it is important to optimize the design of the heat-treat fixtures. The fixture should provide a horizontal loading of the components and should allow a homogenous gas flow around the treated components during quenching as much as possible. Figure 3 shows an example of a fixture made of carbon-reinforced carbon (CFC).

Figure 3: Fixture made of CFC (Source: Schunk GmbH).

In addition, the HPGQ process offers more options for further reduction of heat-treat distortion. These process modifications are explained in the following:

2.1 Dynamic Quenching

Dynamic quenching is a process where the quenching parameters’ gas pressure and/or gas flow velocity are stepwise varied during quenching, see Figure 4. This process is typically divided into three steps [9]:

Step 1: High quenching severity until a certain part-temperature is reached.

Step 2: Quenching severity is reduced for a set time to allow for temperature equalization in the part.

Step 3: Quenching severity is increased again until the end of the quenching process.

Figure 4: Schematic illustration of dynamic quenching for specimen of different sizes.

The control system in the quenching chamber allows to control the different quenching steps of “dynamic quenching” in a very accurate way with a good reproducibility. Optimum results are achieved when using helium. The light-quenching-gas helium can be decelerated and accelerated very precisely for optimum distortion control.

The application of dynamic quenching leads to a reduction of thermal stresses during quenching, and, thus, it offers the potential to reduce heat-treat distortion for certain applications. In addition, a positive effect on fatigue properties can be achieved as well by applying this process modification.

2.2 Reversing Gas flow

High-pressure gas quenching is typically performed with a flow direction from top to bottom through the load. However, modern-gas-quenching chambers offer the possibility to reverse the direction of the gas flow during quenching. Reversing the gas flow means the flow of gas is alternated back-and-forth from top-to-bottom and bottom-to-top. By alternating the gas-flow direction, there is less difference in the cooling curves of parts placed in different layers. This reduces the variation of distortion inside the load.

A schematic view of a quench chamber with reversing gas flow is shown in Figure 5. To allow for the alternating flow direction, the chamber is equipped with flaps operated pneumatically. Depending on the setting of the valves, either top-to-bottom or bottom-to-top flow direction is put into effect. The alternation of the flow direction is time controlled.

Figure 5: Reversing gas flow.

3 Distortion studies

3.1 Comparison of LPC and HPGQ vs. Atmospheric carburizing and Oil quench

Sliding gears made of 8620 material used to be carburized in atmosphere and quenched in oil. For this application, the hardenability of 8620 material was too low to allow for gas quenching. Therefore, the steel grade was changed to 4320H material.

The gears have an outer diameter of 92 mm, an inner diameter of 30 mm, and a height of 24 mm. The specification after heat treatment calls for a surface hardness of 58-64 HRC, a core hardness of 35.1-43.3 HRC, and a case-hardening depth CHD at the pitch of 0.75mm-1.3mm. The microstructure in the case-hardened layer must consist of a minimum of 90% martensite, not more than 10% retained austenite, and no bainite.

For a distortion study, one load with gears made of 8620 material was carburized in atmosphere and oil quenched, and one load made of 4320H material was low-pressure carburized and gas quenched. An image of the LPC-load is in Figure 6.

Figure 6: Load of sliding gears (CFC fixture consisting of 12 layers).

Twenty parts were measured in each load. Figure 7 and 8 show the absolute geometrical values after heat treat, not the change during heat treatment.

Four teeth are measured per each gear. “Helix average” is the average helix value from those four teeth of one gear. Figure 7 shows the average values from 20 measured parts of helix average as well as the maximum and minimum value from those 20 parts for both processes. The spread of “helix average” is clearly reduced with the LPC and HPGQ  process.

Figure 7: Helix average of sliding gears; comparison of atmospheric carburizing and oil quenching vs. LPC and gas quenching.
Figure 8: Helix variation of sliding gears; comparison of atmospheric carburizing and oil quenching vs. LPC and gas quenching.

“Helix variation” is the difference of maximum and minimum helix value from the four measured teeth per each gear. Figure 8 shows the average values of “helix variation” from 20 measured parts as well as the maximum and minimum value of “helix variation” from those 20 parts.

The “helix variation” is strongly reduced when applying LPC and HPGQ, see Figure 8. For the left flank, the average “helix variation” is reduced by 59 percent and, for the right flank, by 48 percent. When applying LPC and gas quenching, the “helix variation” is safely within the maximum tolerance of 50 microns. This offers a significant potential for cost savings in hard machining.

3.2 Size change of pinion gears when applying LPC and HPGQ

The size change of pinion gears was monitored during serial production when applying LPC and HPGQ. The pinion gears are made of SAE 5120H material with an outer diameter of 34 mm, an inner diameter of 20 mm, a height of 15 mm, and a weight of 0.055 kg per part, see Figure 9. The case-hardening depth CHD after heat treatment is specified as 0.5 – 0.8 mm.

Figure 9: Load for heat treatment of pinion gears made of SAE 5120H material.
Figure 10: Size change of inner diameter of pinion gears after LPC and HPGQ; 3 parts measured each from 140 production loads.

Three parts each from 140 production loads were measured. Figure 10 shows the size change of the inner diameter. The inner diameter is shrinking by an average of 39 microns. The shrinking is stable and predictable within a load and from load to load.

Gear shafts made of 20CrMnTi material were analyzed regarding shrinking of the inner diameter at the spline. Figure 11 shows the measurement positions.

Figure 11: Measurement positions for inner spline of a gear shaft.

The shafts have an outer diameter of 48 mm, a height of 233 mm, and a weight of ca. 2.7 kg. The specification after heat treatment calls for a case-hardening depth CHD = 0.6-0.9 mm and a surface hardness of 59-63 HRC.

Twenty shafts were analyzed regarding size change of the inner diameter after applying the process of LPC and gas quenching.

Figure 12 shows the average shrinking and the variation of shrinking at the positions a, b, and c of the inner spline. A homogenous shrinking on the three measurement positions is demonstrated.

Figure 12: Shrinking of the inner spline of a gear shaft on different positions after LPC & HPGQ.

3.3 Optimized fixturing

Final drive ring gears made of 4121 mod material (see Figure 13) were treated with different designs of fixture to improve distortion control. The parts have an outer diameter of 226 mm with 59 external teeth, a height of 32 mm, and a weight of ca. 4.2 kg.

The case-hardening depth CHD is specified as 0.7-1.1 mm, the surface hardness as 64-69 HR45N, and the core hardness is specified to be above 28 HRC.

Figure 13 shows the standard fixture used in serial production. Three new designs of fixturing were tested to improve distortion control.

Figure 13: Final drive ring gear and production load consisting of nine layers.
Figure 14: Change of flatness and change of roundness of final drive ring gears using different fixtures applying LPC and HPGQ (values in mm).

The average change of flatness and average change of roundness are given in Figure 14. With “Fixture 3,” the distortion control was clearly improved:

Change of flatness was reduced by 49%.

Change of roundness reduced by 24% compared to standard fixturing.

As the new design could not be validated in a PPAP (production part approval process), it was not yet possible to implement this improvement into serial production. But it was clearly demonstrated that fixture  design has the potential for improving future distortion control.

3.4 Reversing Gas flow

The following gives an example for the application of the reversing gas flow process as described in Section 2.2. The treated gears are made of 5120 materials, have an outer diameter of 31 mm, a height of 32 mm, and have 24 external teeth, see Figure 15. One load consists of 1,056 pieces treated in nine layers.

Figure 15: Final-drive pinion planetary gear (diameter = 31 mm, 24 teeth).
Figure 16: Reduction of distortion by application of reversing gas flow: comparison between unidirectional and reversing gas flow (helix angle variation of final-drive pinion gears after heat treatment in bottom, middle, and top layer of the load; LF = left flank; RF = right flank).

Figure 16 shows the improvement achieved when introducing the reversing gas-flow process. When applying unidirectional gas flow, the gas is flowing only from top-to-bottom through the load. With reversing gas flow, the flow of gas alternates back-and-forth from top-to-bottom and bottom-to-top, as illustrated in Figure 5. As shown in Figure 16, with unidirectional flow, the parts in the middle and top layer of the load exhibit excessive distortion. With reversing gas flow, the helix angle variations were significantly reduced. For example, for the right flank of the gears from the top layer of the load, the maximum helix angle variation was reduced by 61 percent.

With the optimized reversing gas-flow process, it is not necessary to machine the teeth of these final-drive pinion gears after heat treatment. Only the bores and faces of the gear are machined after heat treatment. This example shows the significant potential to reduce distortion with reversing gas flow.

3.5 Optimized HPGQ-process parameters

The distortion control of drive gears made of 20CrMnTi material was improved by optimizing the HPGQ- parameters. The gears have an outer diameter of 127 mm with 79 external teeth, a height of 12 mm, and weight of ca. 0.3 kg, see Figure 17.

Figure 17: Drive gear.

The specification after heat treatment calls for CHD = 0.5-0.8 mm, a surface hardness of 58-62 HRC, and the core hardness needs to be above 30 HRC.

Figure 18 shows roundness values after LPC and HPGQ. Three sets of quench parameters were tested and 100 pieces were measured in each test.

Figure 18: Roundness of drive gears with different HPGQ parameters.

With “Quench 1,” the gas-flow direction was from top-to-bottom. With “Quench 2,” the gas-flow direction was changed, so the gas is flowing from bottom-to-top. This resulted in a significant reduction of roundness values. With “Quench 3,” the quench intensity was slightly reduced compared to “Quench 2,” which did not, however, result in further improvements.

4 Summary

The LPC (low-pressure carburizing) and HPGQ (high-pressure gas quenching) process offers a significant potential for advanced distortion control. The gas-quenching process provides a more homogenous heat-transfer coefficient on the surface of the quenched components when compared to quenching with liquids such as oil or polymers. In addition, the HPGQ process provides the flexibility to tailor the quench intensity specifically for the needs of the quenched components. The quench intensity can be tailored by defining the quench pressure (from 2 bar to 20 bar) and the gas velocity (from 2 m/s to 20 m/s).

For slide gears, it was demonstrated that distortion control was strongly improved when changing from atmospheric carburizing and oil quenching to LPC and HPGQ. For the left flank, the average “helix variation” was reduced by 59 percent and, for the right flank, by 48 percent. In this application, the steel grade was changed from 8620 material to 4320H material to allow for HPGQ. This change results in higher costs for the material. However, the higher costs of material are overcompensated for by the cost savings in the field of hard machining resulting from the improved distortion control.

The size change of pinion gears was monitored during serial production when applying LPC and HPGQ, demonstrating stable shrinking of the inner diameter within a load and from load to load. On gear shafts, it was demonstrated that a homogenous size change (shrinking) of the inner splines was achieved with LPC and HPGQ.

A distortion study on final drive ring gears showed the importance of fixture design. The change of flatness was reduced by 49 percent and change of roundness was reduced by 24 percent when improving fixture design.

The HPGQ process offers further options such as “dynamic quenching” (variation of the quench intensity during the quench) or “reversing gas flow” (alternating gas flow direction during the quench) to improve distortion control.

The process modification “reversing gas flow” was applied on final drive pinion planetary gears. With reversing gas flow, the flow of gas alternates back-and-forth from top-to-bottom and bottom-to-top. By doing so, the helix angle variations were significantly reduced. For example, for the right flank of the gears from the top layer of the load, the maximum helix angle variation was reduced by 61 percent. 

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